If you are proceeding then go and get 3/4" copper olives, much easier to compress that brass. Gate valves will be useless in a few years if they're not regularly used, if you really want valves then swap them out for lever.
When I restored my place, I replaced the old 3/4" stuff with 22mm as necessary. The olives I used were known as 'converter' types and they were brass with a groove all the way round - this would help the olive compress. They were also coated in a splash of green lacquer.
A 3/4" olive should be just fine in your situation and it should be snug on the pipe. There's a good chance you aren't tightening it up enough.....use two large adjustable spanners, one on the valve body and one on the suspect nut and heave them up.
A gate valve really belongs in the days of steam.....they rely on the sluice principle to make a seal as there is no washer but often don't shut off fully. Having no washer meant they were used on oil supply pipes in the past but it's lever arm type all the way now.
John
If you are proceeding then go and get 3/4" copper olives, much easier to compress that brass. Gate valves will be useless in a few years if they're not regularly used, if you really want valves then swap them out for lever.
Pegler are the make of choice.......originally made in Doncaster and hopefully still are!
Screwfix et al have a good range.
John
3/4" copper olives
Trav Perk or CityPlumbing
I have to say that all your woes would be solved if you used a soldered 3/4" to 22 mm fitting to convert the pipe to 22 mm before it goes into the gate valve.
That is probably what most better plumbers would do!
Of course some would continue with your bodge and add some gas PTFE/ Locktite 55/anaerobic tape and when it weeps again after a couple of days they will not answer their phones!